Recommended application was done by spray regime for two pesticides, namely diniconazole, fenitrothion and a plant growth regulator (gibberellic acid) and their mixtures. Their residues were determined after different successive treatments in and on grape fruits in two consecutive years. The initial deposits of the fungicide diniconazole when used alone were 0.49 and 0.50 ppm for 2006 and 2007, respectively. While the initial deposits of fenitrothion reached to 11.35 and 11.19 ppm for the same interval, respectively. Initial deposits of the plant growth regulator gibberellic acid were 30.52 and 30.42 ppm for the same period, respectively. After mixing the tested pesticides and the plant growth regulator, the initial deposits loss reached 38.77 and 42.0 % for diniconazole, 43.08 and 48.16 % for fenitrothion and 6.88 and 7.00 % for gibberellic acid for the same seasons, respectively. A significant degradation was recorded with the mixture of the two tested pesticides and plant growth regulator compared with that occurred when pesticide was used alone at' the two studied seasons.

Fresh Bolti -fish (Tilpia nilotica) collected randomly from 9 different markets in Ismailia Governorate for evaluation the effect of grilled fish by the method used in grillrooms and houses on the concentration of pesticide residues found and the nutritive value. Results revealed that decrease in the estimated parameters i.e. moisture, crude protein, fat and ash by grilling, this decrease were 6.07, 2.63, 4.07 and 1.56%, respectively. On the contrary, carbohydrates behaved another behavior that there was an obvious increase ranged from 1.98% to 2.92%. Fresh and grilled fish were analyzed to detect 12 organochlorine (OC) and 7 synthetic pyrethroid (SP) pesticides with a mean level on a lipid basis. Gas Liquid Chromatography equipped with Electron Capture Detector GC-ECD was used to detect the contamination in the samples. The results showed that p,p'-DDE isomer was dominated over the other isomers in all analyzed fish samples, followed by q-isomer of hexachlorocyclohexane. The concentrations of OC residues were higher than SP pesticides in all fish muscles. Also, the fresh fish muscle recorded higher concentrations of the evaluated pesticides than the grilled one.