Efficient preparation of carbamates by Rh-catalysed oxidative carbonylation: unveiling the role of the oxidant
2016
Iturmendi, Amaia | Iglesias, Manuel | Munárriz, Julen | Polo, Victor | Pérez-Torrente, Jesús J. | Oro, Luis A.
The synthesis of a wide variety of carbamates from amines, alcohols and carbon monoxide has been achieved by means of a Rh-catalysed oxidative carbonylation reaction that uses Oxone as a stoichiometric oxidant. In-depth studies on the reaction mechanism shed light on the intimate role of Oxone in the catalytic cycle.
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