Step-by-step real time monitoring of a catalytic amination reaction
2019
Thomas, Gilian T. | Janusson, Eric | Zijlstra, Harmen S. | McIndoe, J Scott
The multiple reaction monitoring mode of a triple quadrupole mass spectrometer is used to examine the Buchwald–Hartwig amination reaction at 0.1% catalyst loading in real-time using sequential addition of reagents to probe the individual steps in the cycle. This is a powerful new method for probing reactions under realistic conditions.
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