I2–CF3SO3H Synergistic Promoted sp3 C–H Bond Diarylation of Aromatic Ketones
2012
Zhu, Yan-ping | Jia, Feng-cheng | Liu, Mei-cai | Wu, Liu-ming | Cai, Qun | Gao, Yang | Wu, An-xin
An I₂–CF₃SO₃H synergistic promoted sp³ C–H bond diarylation protocol was developed for the synthesis of 2,2-bis(4-(dimethylamino)phenyl)-1-aryl ethanones. The reaction performed well in the absence of any metal and ligand. It integrated three reactions with different mechanisms (iodination, Kornblum oxidation, and hydroarylation) in a single reactor.
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