Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K₂[(NpO₂)₃B₁₀O₁₆(OH)₂(NO₃)₂]
2010
Wang, Shuao | Alekseev, Evgeny V. | Depmeier, Wulf | Albrecht-Schmitt, Thomas E.
The reaction of Np(v) chloride with molten boric acid results in the disproportionation of Np(v) into Np(iv) and Np(vi), and the crystallization of K₂[(NpO₂)₃B₁₀O₁₆(OH)₂(NO₃)₂]. UV-vis-NIR spectroscopy demonstrates that in addition to the Np(vi) and Np(v) found in the crystal structure, Np(iv) is also present.
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