Syntheses of 3-Oxa-OPC and 2-fluoro-OPC homologues
1998
Toshima, H. (Hokkaido Univ., Sapporo (Japan). Faculty of Agriculture) | Fujino, Y. | Ichihara, A. | Koda, Y. | Kikuta, Y.
Synopsis: 3-Oxa-OPC and 2-fluoro-P-C homologues which do not undergo beta-oxidation were synthesized from esters of odd-numbered OPC homologues by a short-step procedure. The 3-Oxa-OPC homologues were synthesized via etherification of an alcohol with tert-butyl bromoacetate under phase-transfer conditions. The 2-fluoro-OPC homologues were synthesized via the addition of the trichloromethyl anion to an aldehyde and subsequent fluorination
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