Measurement of trace element in Tartary Buckwheat by flame atomic absorption spectrometry with microwave digestion_ | 微波消解火焰原子吸收法测定苦荞中的微量元素___
2011
Chen Yanqin, Chemistry Department of Bijie College in Guizhou Province, Bijie (China)
Chinese. ［目的］采用微波消解火焰原子吸收法测定苦荞中的微量元素。［方法］用HNO3 + H2O2 对苦荞样品进行微波消解处理，采用火焰原子吸收光谱法测定苦荞消解液中的Fe、Cu、Zn、Mn、Mg的含量。［结果］苦荞中Mg的含量较高；各元素的回收率为94.8%~101.5%，结果满意。［结论］该法简便、快速、准确，有良好的重现性，能满足日常分析检测的需要。_
Show more [+] Less [-]English. ［Objective］ The research aimed to measure the trace element in Tartary buckwheat by the flame atomic absorption spectrometry with microwave digestion. ［Method］ Tartary buckwheat sample was carried out the microwave digestion by HNO3 + H2O2. The flame atomic absorption spectrometry was used to measure the contents of Fe, Cu, Zn, Mn and Mg in the digestion solution of Tartary buckwheat. ［Result］ Mg content was higher in Tartary buckwheat. The recovery ratio of each element was during 94.8%-101.5%, and the result was satisfactory. ［Conclusion］ The method was simple, convenient, quick and accurate. It had the good repeatability and could satisfy the requirement of routine analysis and detection.
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