Synthesis of Geminal Azido–Halo Compounds and α-Azidoalkyl Esters from Aldehydes via α-Azido Alcohols
2017
Banert, Klaus | Berndt, Christian | Weigand, Kevin
α-Azido alcohols are generated by treating aldehydes with hydrazoic acid in chloroform. These adducts are transformed into geminal azido–halo compounds through the reaction with phosphorus trichloride or phosphorus tribromide, whereas α-azidoalkyl esters are isolated after interaction with acyl chlorides.
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