Evaluation of the Mineral Content in Forage Palm (Opuntia ficus-indica Mill and Nopalea cochenillifera) Using Chemometric Tools
2021
Santana, Filipe B. | Silveira, Hilária F. A. | Souza, Laís A. | Soares, Sarah Adriana R. | de Freitas Santos Júnior, Aníbal | Araujo, Rennan Geovanny O. | Santos, Daniele Cristina M. B.
An acid digestion procedure of the forage palm (Opuntia ficus-indica Mill and Nopalea cochenilifera) employing a closed digestor block applied full 2⁴ factorial design was optimized. The optimal conditions were HNO₃ 5.0 mol L⁻¹, 2.0 mL of H₂O₂ 30% m m⁻¹, 120 min of digestion, and heating temperature of 180 °C. The certified reference materials of apple leaves (NIST 1515) and tomato leaves (Agro C1003a) were used to evaluate the accuracy of the analytical method. The concentrations of the macroelements were (in % m m⁻¹) Ca (1.32–3.71), K (0.88–5.29), Mg (0.70–1.78), and P (0.03–0.32). For the microelements, the concentrations (in μg g⁻¹) obtained were As (< 1.39), Cd (< 0.10), Cu (< 0.17–5.6), Fe (8.0–50.2), Na (< 1.85), Sr (41–348), and Zn (17.3–159). Essential elements such as Ca, Mg, and Zn made good contributions to daily intake, being an alternative to meet the nutritional needs of these macroelements and microelements in humans. Principal component analysis (PCA) and hierarchical cluster analysis (HCA) were used to evaluate the results, obtaining trends between the samples in relation to their mineral composition.
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