Synthesis and resolution of 2-amino-5-aza[6]helicene
2022
Bhalodi, Esha H. | Patel, Krupa N. | Bedekar, Ashutosh V.
The synthesis of 2-amino-5-aza[6]helicene and its derivatives is reported. The diastereomeric (R)-menthylcarbamate derivative of this aza[6]helicene is prepared and its isomers were physically separated by column chromatography and their optical properties were measured. Optically pure isomer (P)-2-amino-5-aza[6]helicene was generated and its Boc-derivative was prepared.
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