Use of the enantiomeric composition for the assessment of the authenticity of fruit beverages
2003
Ruiz del Castillo, M. Luisa | Caja, Maria del Mar | Herraiz Carasa, Marta | Comisión Interministerial de Ciencia y Tecnología, CICYT (España)
Enantiomeric compositions of chiral terpenes in commercial fruit beverages were examined by solid phase microextraction−gas chromatography (SPME-GC). Optimization of the method was accomplished on the basis of some parameters involved in the extraction, such as heating temperature and extraction time, that provided the highest peak areas, 60 °C and 2 min being the optimal values. With the proposed method relative standard deviation (RSD) values from three replicates ranging from 2 to 12% were obtained. The enantiomeric distribution of some terpenes remained constant, whereas other terpenes (linalool, terpinen-4-ol, and α-terpineol) exhibited a considerable variation among samples. This can be indicative of the eventual addition of aromas to some fruit beverages.
Show more [+] Less [-]This work was financially supported by CICYT (Project ALI99-1188).
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