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Behavior of EPN with mice to explain the sudden death of Bombycille
1999
Yamamoto, A. (Nagano-ken. Research Inst. for Health and Pollution (Japan)) | Tsukioka, T. | Yoshida, T. | Sato, M. | Maruyama, S.
Determination of aliphatic lower amines in environmental samples
1999
Tsukioka, T. (Nagano-ken. Research Inst. for Health and Pollution (Japan))
A micro analytical method has been established for aliphatic lower primary and secondary amines in environmental water and sediment. Amines were distilled and allowed to react with benzenesulfonyl chloride under an alkaline condition. The derivatized compounds were extracted with benzene under an acidic condition and subjected to a determination by GC/MS. This method has been successfully applied for a simultaneous determination of primary and secondary amines with recovery over 80%, except for methylamine, and C.V. below 7%, except for methyl and dimethyl amines; moreover, the detection limit were 0.1 micro g/L for all of the amines determinated. This method is excelent also in sensitivity, is sufficiently applicable to environmental samples.
Show more [+] Less [-]Survey of chemical substances in freshwater fish
1999
Terasawa, J. (Nagano-ken. Research Inst. for Health and Pollution (Japan)) | Miyagawa, A. | Tsukioka, T. | Sato, M.
Behavior of airborne halocarbons in urban and highland areas of Nagano prefecture [Japan]
1999
Sasai, H. (Nagano-ken. Research Inst. for Health and Pollution (Japan)) | Katsuno, T. | Nomizo, H. | Satsumabayashi, H.
Examination of the similarity of change of patient's number among the areas in Japan using surveillance data
1999
Wada, M. (Nagano-ken. Research Inst. for Health and Pollution (Japan))
Fauna and seasonal fluctuation of house dust mites in Nagano prefecture [Japan]
1999
Nakamura, K. (Nagano-ken. Research Inst. for Health and Pollution (Japan)) | Takaoka, M.
Determination of pyrimidifen in agricultural products by GC/MS
1999
Tsukioka, T. (Nagano-ken. Research Inst. for Health and Pollution (Japan)) | Terasawa, J. | Miyagawa, A. | Sato, M.
A method by GC/MS has been established for the determination of Pyrimidifen in agricaltural products. The Pyrimidifen in agricultural products is extracted with acetone, concentrated, and extracted with n-hexane. The solution is cleaned up with a Florisil column and subjected to a determination by GC/MS using p-terphenyl-d14 as the internal standard. This method is featured by the recovery over 80 % with its C .V. below 8 % and the detection limit 1 micro g/kg. This method, excellent in sensitivity and selectivity, is useful as a rutine analytical method for agricultural products.
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