DEVELOPING AND VALIDATION OF METHOD FOR DETECTION OF QUINOLONE RESIDUES IN POULTRY MEAT
2010
Stoilova, N., Central Laboratory of Veterinary-Sanitary Investigation and Ecology, Sofia (Bulgaria) | Petkova, M., Central Laboratory of Veterinary-Sanitary Investigation and Ecology, Sofia (Bulgaria)
The objective of this study was to present simple, rapid and applicable HPLC-method with fluorescence detection for determination of quinolone-residues in chicken muscle. Presence of antibacterial residia gives reise to risk for health, because of chance by disease, allergy or cancer effect. The residues of ciprofloxacine, enrofloxacine, norfloxacine, danfloxacine, difloxacine, sarafloxacine, oxolinic acid, nalidixic acid and flumequine are extracted with acetonitril. The extract was cleaned with an SPE - procedure with HLB cartridges. Elute was analyzed via Zorbax Eclipse XDB liquid chromatography column. It was used gradient program for eluting and time table program because of the different wave lengths of excitation and emission.
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