Electrochemical formation of Mnᴵᴵᴵ-peroxo complexes supported by pentadentate amino pyridine and imidazole ligands
2013
El Ghachtouli, Sanae | Vincent Ching, H. Y. | Lassalle-KaiserPresent address: Synchrotron Soleil, L'Orme des Merisiers, Saint-Aubin – BP 48, 91192 Gif-sur-Yvette, France. Benedikt | Guillot, Régis | Leto, Domenick F. | Chattopadhyay, Swarup | Jackson, Timothy A. | Dorlet, Pierre | Anxolabéhère-Mallart, Elodie
A novel and efficient method for preparing [Mnᴵᴵᴵ(O₂)(L)]⁺ complexes using electrochemically generated superoxide is reported, with the reaction probed by low temperature electronic absorption and electron paramagnetic resonance spectroscopic techniques.
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