TiO2/g-C3N4 photocatalyst for the purification of potassium butyl xanthate in mineral processing wastewater
2021
Zhang, Minghui | Han, Ning | Fei, Yawen | Liu, Jiaojiao | Xing, Lingbao | Núñez Delgado, Avelino | Jiang, Man | Lau, R. S. M. (Ronald S. M.)
In the present work, TiO₂-graphite-phase-carbon-nitride (TiO₂/g-C₃N₄) was prepared through a hydrothermal method to obtain a new photocatalytic material. This material was characterized by means of scanning electron microscope (SEM), transmission electron microscope (TEM), X-ray energy spectrometer (EDS), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared spectroscopy (FT-IR), Solid-state UV–Vis diffuse reflectance spectrometry (UV–Vis-DRS) and electron paramagnetic resonance (EPR). The synthesized TiO₂/g-C₃N₄ exhibited homogeneous morphology, in which TiO₂ nanoparticles were uniformly distributed on the g-C₃N₄ nanosheets. Regarding its potential use as photocatalytic material in the treatment of mineral processing wastewater, 18% TiO₂/g-C₃N₄ showed superior photodegradation performance than TiO₂ and g-C₃N₄, to give 97.1% degradation rate under 100 min of simulated light irradiation. The experimental results showed that the successful incorporation of TiO₂ on g-C₃N₄ nanosheets enhanced the spectral response range of TiO₂/g-C₃N₄, and the photocatalytic activity was improved. In view of that, it can be considered that this kind of photocatalytic material has a good prospect in the treatment of mineral processing wastewater, which would have clearly environmental relevance.
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