Supercritical fluid extraction with reflux for citrus oil processing
1997
Sato, M. | Goto, M. | Kodama, A. | Hirose, T.
Terpenes in citrus oil must be removed to stabilize the products and to dissolve it in aqueous solution. Supercritical fluid extraction has been investigated for the terpeneless citrus oil processing as a lower temperature process. In order to achieve higher yield and higher separation selectivity, a continuous countercurrent extraction with reflux was studied at a temperature of 333 K and a pressure of 8.8 MPa. Cold-pressed orange oil from Brazil and a model mixture of 80% limonene and 20% linalool, where limonene and linalool are principal constituent of terpenes and oxygenated compounds in orange oil, were used as feed and carbon dioxide was used as solvent. Operation at total reflux was carried out to calculate the minimum number of plates required to achieve a separation between limonene and linalool. Effects of the solvent-to-feed ratio, reflux ratio, and feed inlet position on the yield and selectivity were investigated for continuous operation. The selectivity increased with the increase in the solvent-to-feed ratio. Terpeneless citrus oil was obtained on the operation at the higher solvent-to-feed ratio and longer stripping section.
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