Enantiospecific Total Synthesis of Macrolactone Sch 725674
2014
Bali, Amit K. | Sunnam, Sunil K. | Prasad, Kavirayani R.
The enantiospecific total synthesis of 14-membered macrolactone Sch 725674 was accomplished from tartaric acid. Key reactions in the synthesis include the Ley’s dithiaketalization of an alkynone derived from the bis-Weinreb amide of tartaric acid, Boord olefination, and ring-closing metathesis of an acrylate ester.
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