Optimization of Algerian Thymus fontanesii Boiss. and Reut Essential Oil Extraction by Electromagnetic Induction Heating
2018
Lamia Sid Ali, Laboratoire de Valorisation des Substances Naturelles, Universite Djilali Bounaama de Khemis-Miliana, Algeria | Moussa Brada, Laboratoire de Valorisation des Substances Naturelles, Universite Djilali Bounaama de Khemis-Miliana, Algeria | Marie-Laure Fauconnier, Gembloux Agro Bio Tech Universite de Liege, Gembloux, Belgium | Tierry Kenne, Gembloux Agro Bio Tech Universite de Liege, Gembloux, Belgium
The present study deals with the determination of optimal values of operating parameters such as the temperature of heating, the mass of the plant material and the volume of water leading to the best yield of electromagnetic induction (EMI) heating extraction of Algerian Thymus fontanesii essential oil. After an appropriate choice of the three critical variables, eight experiments leaded to a mathematical model as a first-degree polynomial presenting the response function (yield) in the relation to the operating parameters. From the retained model, we were able to calculate the average response, the different effects and their interactions. The maximum of essential oil recovery percentage relative to the initial mass of plant material was 1.69%, and was obtained at (140 ℃, 250 g and 4.5 L). The chemical composition of the Algerian T. fontanesii essential oil under the obtained optimal conditions (140 ℃, 250 g and 4.5 L), determined by GC/MS and GC/FID, reveled of the presence of major components such as: carvacrol (70.6 ± 0.1%), followed by p-cymene (8.2 ± 0.2%).
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