Continuous flow Suzuki–Miyaura couplings in water under micellar conditions in a CSTR cascade catalyzed by Fe/ppm Pd nanoparticles
2020
Wood, Alex B. | Nandiwale, Kakasaheb Y. | Mo, Yiming | Jin, Bo | Pomberger, Alexander | Schultz, Victor L. | Gallou, Fabrice | Jensen, Klavs F. | Lipshutz, Bruce H.
The first demonstration of aqueous surfactant-enabled Suzuki–Miyaura couplings run under flow conditions is described. In addition, use of an even more challenging heterogeneous nanoparticle catalyst, containing only 800 ppm of Pd (i.e., 0.08 mol%) in the form of Fe/ppm Pd nanoparticles, is sufficient using a continuous stirred-tank reactor (CSTR).
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