Solvent-free on-surface synthesis of boroxine COF monolayers
2017
Spitzer, Saskia | Rastgoo-Lahrood, Atena | Macknapp, Klaus | Ritter, Viktoria | Sotier, Stefan | Heckl, Wolfgang M. | Lackinger, Markus
A protocol is proposed for the solvent-free on-surface synthesis of covalent organic framework monolayers by condensation of diboronic acids. Monomers are vapor-deposited and water is used for equilibrium regulation. Samples are characterized on progressively smaller length scales by light microscopy, Scanning Electron Microscopy, and Scanning Tunneling Microscopy.
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