Thiocarbonyl induced heterocumulenic Pauson–Khand type reaction: expedient synthetic method for thieno[2,3-b]indol-2-ones
2007
Saito, Takao | Nihei, Hiroshi | Otani, Takashi | Suyama, Toshiyuki | Furukawa, Naoki | Saito, Masatoshi
The first examples of CS induced Pauson–Khand type reactions are described; 2-alkynylphenyl isothiocyanates were converted to 3-substituted-2H-thieno[2,3-b]indol-2-ones in the presence of a stoichiometric amount of Mo(CO)₆ or Co₂(CO)₈, or a catalytic amount of Rh catalyst under an atmospheric pressure of carbon monoxide.
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