O,O-Diethyl dithiophosphoric acid mediated direct synthesis of thioamides from aldehydes and ketones
2012
Yadav, Arvind K. | Srivastava, Vishnu P. | Yadav, Lal Dhar S.
A general and convenient method for a one-pot conversion of aldehydes and ketones into thioamides has been developed. The protocol involves oximation of aldehydes and ketones followed by deoxygenative thioamidation of oximes with O,O-diethyl dithiophosphoric acid which acts as an acid as well a source of sulfur. The method is operationally simple, high yielding, and also applicable to the conversion of amides and nitriles into the corresponding thioamides.
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