C₁₈, C₈, and perfluoro reversed phases on diamond for solid-phase extraction
2009
Saini, Gaurav | Wiest, Landon A. | Herbert, David | Biggs, Katherine N. | Dadson, Andrew | Vail, Michael A. | Linford, Matthew R.
In spite of advances in solid-phase extraction (SPE) technology there are certain disadvantages to current SPE silica-based, column packings. The pH range over which extraction can occur is limited and each column is generally only used once. New diamond-based reversed SPE phases (C₁₈, C₈, and perfluorinated) were developed in our laboratories. Studies were done which show that these phases do not have the same limitations as traditional silica-based stationary phases. The synthesis and properties of these diamond-based phases are presented, and the stability, percent recovery, and column capacity are given for the C₁₈ phase.
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