Data acquisition of triple quadrupole LC-MS for the citrinin determination
Vuković, Gorica Lj. (Institute for Public Health of Belgrade, Belgrade (Serbia)) | Bursić, Vojislava P. (Faculty of Agriculture, Novi Sad (Serbia)) | Aleksić, Goran A. (Institute for Plant Protection and Environment, Belgrade (Serbia)) | Kuzmanović, Slobodan T. (Institute for Plant Protection and Environment, Belgrade (Serbia)) | Cara, Magdalena X. (Faculty of Agriculture and Environemnt, Tiranë (Albania)) | Abd El-Wahab, Rania Ahmed (Plant Protection Research Institute, Giza (Egypt). Agriculture Research Center)
The analysis of citrinin is challenging because it needs to be detected in low concentrations in complex sample matrices. Before citrinin quantification, the data acquisition of LC-MS/MS must be performed, which includes the determination of ion monitoring reaction (SRM), finding fragmentation energies (Frag.) and collision cell energies (CE) for which the response of citrinin will be the highest for the given conditions. The best response of citrinin is obtained for Frag. of 66 V and CE of 17 and 29 V
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