Oxidation of disulfides with Selectfluor™: concise syntheses of thiosulfonates and sulfonyl fluorides
2011
Kirihara, Masayuki | Naito, Sayuri | Ishizuka, Yuki | Hanai, Honoka | Noguchi, Takuya
The reaction of aromatic or benzylic disulfides with 2.5equiv of Selectfluor™ in acetonitrile/water (10:1) at room temperature efficiently produced the corresponding thiosulfonates. On the other hand, the reaction of disulfides with 6.5equiv of Selectfluor™ in refluxing acetonitrile/water (10:1) provided sulfonyl fluoride in high yields.
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