Homogeneity study of a corn flour laboratory reference material candidate for inorganic analysis
2015
dos Santos, Ana Maria Pinto | dos Santos, Liz Oliveira | Brandao, Geovani Cardoso | Leao, Danilo Junqueira | Bernedo, Alfredo Victor Bellido | Lopes, Ricardo Tadeu | Lemos, Valfredo Azevedo
In this work, a homogeneity study of a corn flour reference material candidate for inorganic analysis is presented. Seven kilograms of corn flour were used to prepare the material, which was distributed among 100 bottles. The elements Ca, K, Mg, P, Zn, Cu, Fe, Mn and Mo were quantified by inductively coupled plasma optical emission spectrometry (ICP OES) after acid digestion procedure. The method accuracy was confirmed by analyzing the rice flour certified reference material, NIST 1568a. All results were evaluated by analysis of variance (ANOVA) and principal component analysis (PCA). In the study, a sample mass of 400mg was established as the minimum mass required for analysis, according to the PCA. The between-bottle test was performed by analyzing 9 bottles of the material. Subsamples of a single bottle were analyzed for the within-bottle test. No significant differences were observed for the results obtained through the application of both statistical methods. This fact demonstrates that the material is homogeneous for use as a laboratory reference material.
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