Quantitative LC/MS-MS determination of sulfonamides and some other antibiotics in honey
2002
Kaufmann, A. | Roth, S. | Ryser, B. | Widmer, M. | Guggisberg, D.
A simple and rapid method was developed for the determination of 20 antibiotics (sulfonamides, tetracyclines, and flumequine) in honey by liquid chromatography tandem mass spectrometry. The proposed method is sensitive (limit of detection 0.5 to 10 ppb for the various antibiotics) and selective. A hydrolysis step ensures the liberation of sugar-bound sulfonamides. The approach has been used to analyze some 300 honey samples. A number of them were found to have exceeded the Swiss limit of 50 ppb.
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书目信息
Journal of AOAC International
卷
85
期
4
页码
853
- 860
ISSN
1060-3271
出版者
John Wiley & Sons, Ltd
其它主题
Flumequine; Liquid chromatography; Liquid; Anti-infective agents; Reference standards; Anti-infective agents
语言
英语
注释
2019-12-05
类型
Journal Article; Text
2024-02-27
MODS