Improved synthesis and spectral characterization of D5281, an oxadiazine miticide/insecticide

Dekeyser, M.A.; Mitchell, D.S.; Downer, R.G.H.

Improved synthesis and spectral characterization of D5281, an oxadiazine miticide/insecticide

1994

Dekeyser, M.A. | Mitchell, D.S. | Downer, R.G.H.

An improved synthesis of the novel dihydrooxadiazine pesticide D5281 was obtained, resulting in a yield increase from 19 to 60%. The structure of D5281 was characterized by carbon-13 and high-field proton NMR spectroscopy and mass spectrometry. The evidence is consistent with and therefore supports the proposed structure.

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