Topochemical mechanoactivated phosphonylethynylation of pyrroles with chloroethynylphosphonates on solid Al2O3 or K2CO3 media
2015
Gotsko, Maxim D. | Sobenina, Lyubov’ N. | Tomilin, Denis N. | Ushakov, Igor’ A. | Dogadina, Albina V. | Trofimov, Boris A.
Dialkyl 2-(1H-pyrrol-2-yl)ethynylphosphonates have been synthesized from their respective pyrroles by a transition metal-free, topochemical mechanoactivated phosphonylethynylation (room temperature, 24–48h) using chloroethynylphosphonates on solid Al2O3 (40–58% yield) or K2CO3 (38–43% yield).
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书目信息
Tetrahedron letters
卷
56
期
32
页码
4657
- 4660
ISSN
0040-4039
出版者
Elsevier Ltd
其它主题
Pyrroles; Chloroethynylphosphonate; Ethynylation; Pyrrole; Potassium carbonate; Ambient temperature; K2co3; Aluminum oxide; Al2o3
语言
英语
类型
Journal Article; Text
2024-02-28
MODS
