Urban Heat Island (UHI) is a common urban problem associated with a wide variety of factors, including air pollution. This study investigated the relationship between Land Surface Temperature (LST) and air pollution as two spatial phenomena affecting urban areas. LST was estimated from OLI sensor images taken on 01/07/2020 using the single-channel algorithm. Air pollution was assumed to be indicated by the concentrations of NOX, NO2, NO, PM2.5 and SO2, which were obtained by Inverse Distance Weighting (IDW) interpolation from the data recorded on the same date as satellite images. Correlations were measured in terms of R and R2 and errors were estimated in terms of RMSE, MAE and MBE. The highest R and R2 were obtained for SO2 (20.89 and 45.99, respectively). The results showed that despite the high correlation between SO2 and LST, PM2.5 has a much better error distribution. Therefore, further research should be conducted on the relationship between these indices.