Notizen: Phosphoranes with a Chiral Centre Containing the 1,2-Oxaphosphetane Ring System
2014
Gibson, James Andrew | Röschenthaler, Gerd-Volker | Schmutzler, Reinhard
Hexafluoroacetone and tetramethyldiphosphine react readily at low temperatures producing three 4,4-bis(trifluoromethyl)-1,2-oxaphosphetanes (1), (2), and (3). The compounds have chiral centres at phosphorus producing doubling of resonances in the NMR spectra.
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