The aroma of coffee is the main quality factor. Compounds with floral, fruity, citrus and sometimes fermented aroma notes are defined as high quality characteristics for the specialty coffee brew. Commercial coffees mostly are at medium roast and the aroma profile is focused on balanced chocolate, caramel, toasted bread and almond bitterness aroma notes. These sensory characteristics set the focus for volatile compound profile analysis by Headspace solidphase microextraction (HS-SPME). The most popular fibres for commercial coffee aroma profile analysis are DVB/ CAR/PDMS, CAR/PDMS, PDMS/DVB and PA. There is limited research done about specialty coffee aroma profile and evaluation of more suitable fibres for solid-phase microextraction. The aim of the research is to evaluate the aroma composition of specialty coffee brews using different SPME fibres. Results demonstrated that CAR/PDMS fibre, compared to other fibres, can extract significantly more volatile compounds with higher peak areas in all chemical compound groups, except phenols. The CAR/PDMS was the only fibre which could detect all 17 important volatile compounds for specialty coffee. In conclusion, from the given research evidence, CAR/PDMS fibre is suggested as the most suitable SPME fibre coating for volatile compound extraction for specialty coffee brew import. The result provides evidence for improved specialty coffee aroma profile analysis by SPME.