Air pollution can be defined as the accumulation of gas, air, or particulate matter released as a result of fuel residues and chemical processes in the atmosphere in amounts that harm the lives of living things. Rapid urbanization, industrialization, increase in the number of motor vehicles, meteorological conditions, fuels used for heating, and the spread of industrial establishments and thermal power plants play an important role in the increase in air pollution. Air pollution is a major environmental problem affecting people in both developed and developing countries, and it is estimated that megacities in developing countries, and a quarter of the world's population are exposed to unhealthy concentrations of air pollutants. People living in cities with high outdoor air pollution are more likely to suffer from heart disease, respiratory problems, and lung cancer than those living in urban areas with clean air. In the industrialized western world, urban air pollution is in some respects in its final stages, with a dramatic decline in SO2 and soot levels. The increase in the number of private vehicles is a newly emerging problem. Rapid urbanization in most developing countries has so far led to uncontrolled growth and environmental degradation. Air pollution levels are still rising in many cities. In this study, air quality was tried to be measured along Dr. Sami Yağız Street, which is one of the most heavily used areas of Niğde. H2S, O2 and CO measurements were made at 25 points at equal intervals on both sides of the street. Measurements were made at a total of 4 different time periods per day. The obtained values were transferred to ArcGIS 10.3 software and maps were produced. Measurement of gases other than H2S is not distributed homogeneously along the street, and traffic density and the businesses on the sides of the street cause changes in the rates of the gases.