In this work, the effects of refrigerator freezing method (RF), spiral tunnel freezing method (SF), and liquid nitrogen spray freezing method (LF) on water distribution, microstructure, retrogradation, and digestion properties of Liangpi are investigated. Results from SEM and water distribution show the starch gel structure of Liangpi after LF treatment is more continuous, and its A₂₁ content is higher, which are closer to fresh Liangpi, followed by SF and RF. XRD and FT‐IR data indicate that as the freezing rate increases, the relative crystallinity and R₁₀₄₇/₁₀₂₂ value of the samples decrease. This is consistent with the data obtained from texture properties. Texture properties of samples treat by LF and SF are closer to fresh Liangpi, especially the hardness index. The in vitro digestibility of Liangpi also shows the same trend. Therefore, the freezing method with a faster rate could inhibit the starch gel retrogradation, improve the texture properties of Liangpi, and guarantee the quality of Liangpi. However, considering the economics of enterprise production, the spiral tunnel freezing method is more suitable for the actual production of frozen Liangpi. The data obtained provide a theoretical guidance for the actual production of frozen Liangpi.

The addition of dietary fibers can alleviate the deteriorated textural properties and water binding capacity (WBC) that may occur when the fat content is lowered directly in the formulas of comminuted meat products. This study investigated the effects of the addition of chitosan or carboxymethyl cellulose (CMC) (2% w/w) to a model meat product. Both dietary fibers improved the water-binding capacity (WBC), while chitosan addition resulted in a firmer texture, CMC lowered the hardness. Chitosan addition resulted in a 2-fold reduction of lipid oxidation products, whereas CMC had no significant effect on oxidation. The effect of chitosan addition on lipid oxidation was evident both in the meat system and after simulated in vitro gastrointestinal digestion. Low-field nuclear magnetic resonance (NMR) relaxometry revealed that the fibers impacted the intrinsic water differently; the addition of chitosan resulted in a faster T₂ relaxation time corresponding to water entrapped in a more dense pore network. Coherent anti-Stokes Raman scattering (CARS) microscopy was for the first time applied in a meat product to study the microstructure, which revealed that the two fibers exerted different effects on the size and entrapment of fat droplets in the protein network, which probably explain the mechanisms by which chitosan reduced lipid oxidation in the system.