Facile access to 3,5-symmetrically disubstituted 1,2,4-thiadiazoles through phosphovanadomolybdic acid catalyzed aerobic oxidative dimerization of primary thioamides
2014
Yajima, Kazuhisa | Yamaguchi, Kazuya | Mizuno, Noritaka
In the presence of Keggin-type phosphovanadomolybdic acids, e.g., H₆PV₃Mo₉O₄₀, oxidative dimerization of various kinds of primary thioamides including aromatic, heterocyclic, and aliphatic ones efficiently proceeded to give the corresponding 3,5-disubstituted 1,2,4-thiadiazoles in excellent yields.
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